CN103070473A - Electronic cigarette tobacco juice prepared from faint scent tobacco leaves - Google Patents

Electronic cigarette tobacco juice prepared from faint scent tobacco leaves Download PDF

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Publication number
CN103070473A
CN103070473A CN2013100297032A CN201310029703A CN103070473A CN 103070473 A CN103070473 A CN 103070473A CN 2013100297032 A CN2013100297032 A CN 2013100297032A CN 201310029703 A CN201310029703 A CN 201310029703A CN 103070473 A CN103070473 A CN 103070473A
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China
Prior art keywords
tobacco
faint scent
electronic cigarette
tobacco leaf
cured tobacco
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CN2013100297032A
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Inventor
杨建云
巩效伟
张伟
胡巍耀
王欣林
朱东来
周博
颜克亮
杨丽萍
陈江红
张天栋
李庚�
宫玉鹏
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Hongyun Honghe Tobacco Group Co Ltd
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Hongyun Honghe Tobacco Group Co Ltd
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Priority to CN2013100297032A priority Critical patent/CN103070473A/en
Publication of CN103070473A publication Critical patent/CN103070473A/en
Pending legal-status Critical Current

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Abstract

The invention discloses electronic cigarette tobacco juice prepared from faint scent tobacco leaves. The electronic cigarette tobacco juice is prepared by uniformly mixing 10 to 30 percent of faint scent flue-cured tobacco leave extract, 5 to 10 percent of tobacco flavor, 1 to 5 percent of tobacco perfume, 5 to 10 percent of deionized water, 10 to 20 percent of glycerol and the balance of propylene glycol. The faint scent flue-cured tobacco leave extract is one of a Yunnan faint scent flue-cured tobacco leave extract and a Fujian faint scent flue-cured tobacco leave extract, or a mixture of the Yunnan faint scent flue-cured tobacco leave extract and the Fujian faint scent flue-cured tobacco leave extract. The electronic cigarette tobacco juice takes a faint scent tobacco leave extract as a main component, so that the aroma and mouthfeel of an electronic cigarette are close to those of the traditional faint scent cigarette. The electronic cigarette tobacco juice is used for atomizing the electronic cigarette and does not generate tar and CO, the harm to consumers is greatly reduced and the product cannot generate the harm of passive smoking.

Description

A kind of tobacco juice for electronic smoke that utilizes the preparation of delicate fragrance type tobacco leaf
Technical field
The invention belongs to the electronic cigarette technical field, specifically relate to a kind of tobacco juice for electronic smoke that utilizes the preparation of delicate fragrance type tobacco leaf.
Background technology
Along with the development of global Tobacco Control campaign, the cigarette living environment is increasingly serious, and in order to satisfy different consumer demands, the product of various simulation cigarette continues to bring out, wherein with smokeless tobacco and the most extensive without the burning cigarette." smokeless tobacco " refers in incombustible situation, by the tobacco of oral cavity or nasal cavity consumption, for example snuff and quid, however the consumer is except the nicotine demand, the sensation of " cloud and mist of handling up " when needing to smoke to a great extent, it is not very popular therefore having caused smokeless tobacco.Refer in incombustible situation without the burning tobacco, realize the dual satisfied of nicotine and fragrance by certain γ-ray emission.Mainly containing at present electrical heating cigarette (EHP), carbon heating cigarette (CHP) and electrospray cigarette (e-Cig) is electronic cigarette.
Electronic cigarette is the electronics conveyer that transmits nicotine by the electrons heat means to respiratory system.As the cigarette substitute, electronic cigarette is extremely similar to real cigarette on external form.Its simulated cigarette taste does not but have cigarette ash, does not fall cigarette end, does not burn, and does not have naked light, does not contain the harmful substances such as tar, carbon monoxide, hydrogen cyanide, methacrylaldehyde, arsenic, lead, mercury.In addition, nicotine solution forms aerosol after atomizing, and aerosol is diluted rapidly in air, can not form second-hand-cigarette.This electronic cigarette that integrates modern microelectric technique, biotechnology, healthy living theory has firmly been held consumer's psychological characteristics, has attracted at short notice numerous consumer's eyeballs of giving up smoking wanted.
Because the numerous advantage of electronic cigarette, increasing consumer begins to accept and use electronic cigarette, and the some shortcomings part of electronic cigarette also progressively manifests.According to investigations research, electronic cigarette is compared with cigarette, although the perceptual image cigarette such as shape, feel, smog, but the smog that the electronic cigarette liquid that is used for these electronic cigarettes produces is at aspects such as fragrance, tastes, larger with real cigarette perceptual difference distance, especially the product that forms with various essence and flavoring agent allotments, the consumer is difficult to accept or be accustomed to its fragrance and taste.These deficiencies have affected the quality of electronic cigarette greatly, also restricting simultaneously electronic cigarette popularize and popular.And the tobacco juice for electronic smoke that extracts, prepares according to flue-cured tobacco flavor types there is not yet report.
Flue-cured tobacco flavor types is the important evidence that quality of tobacco evaluation and cigarette composition are used, and as far back as the sixties in 20th century, Zhu Zunquan, Wang Chenghan etc. just is divided into China's tobacco leaf delicate fragrance type, middle odor type, Luzhou-flavor three large odor types.The tobacco leaf odor type determines by the several factors acting in conjunction, except with hereditary capacity mutually outside the Pass, also relevant with weather, landform, soil and alcoholization modulation.The odor type of flue-cured tobacco is the important composition factor of Chinese-style cigarette style, is the important sign of tobacco style characteristic, is to carry out the important evidence that the quality of tobacco zone is divided, and is the important indicator of working out production technology measures, execution standardization production.Therefore, no matter be cigarette industry or tobacco leaf producing region, no matter be the producer of tobacco leaf or the user of tobacco leaf, all the odor type of flue-cured tobacco is given the attention of height, tobacco leaf odor type problem also is the focus of characteristic tobacco research and development.The long-term practice of industrial application proves, delicate fragrance type tobacco leaf producing region mainly take Yunnan, Fujian is representative.Each tobacco leaf producing region inherent quality of tobacco leaf smoking result is roughly as follows:
Yunnan tobacco: delicate fragrance type fragrance, inhale flavor clean, little pleasantly sweet, smoke concentration is lighter, and region are mixed, and gas is little to be had, and to slightly large, excitant is larger in the strength, and flammability is strong, and grey is white.
The Fujian tobacco leaf: delicate fragrance type fragrance, inhale flavor clean, little pleasantly sweet, the tobacco is very mild, and region are mixed, and gas is little to be had, and excitant is lighter, and flammability is medium, and grey is black.
As the delicate fragrance type tobacco leaf of one of three large odor types, it is interpreted as " have outstanding delicate fragrance fragrance smell, make people's grace that feels pleasure "; " fragrance of flue-cured tobacco own is arranged, but not strong, have simultaneously pleasant outstanding fragrance ".The delicate fragrance type tobacco leaf is take Yunnan Tobacco as representative, and the Fujian tobacco leaf is the delicate fragrance with another feature.Tobacco juice for electronic smoke of the present invention is exactly to be produced the extraction of delicate fragrance type cured tobacco leaf, to be prepared from by national high-quality delicate fragrance type tobacco leaf producing region, preferably resolves the electronic cigarette tobacco leaf in the gap of the aspect such as fragrance, mouthfeel and cigarette.
Summary of the invention
The object of the invention is to for existing tobacco juice for electronic smoke in the deficiency aspect the suction sensations such as fragrance, mouthfeel, a kind of tobacco juice for electronic smoke that utilizes the preparation of delicate fragrance type tobacco leaf is provided, the application of this tobacco juice can improve the inherent suction quality of electronic cigarette, make electronic cigarette more near fragrance, the taste of cigarette, more can cater to consumer's needs.
Purpose of the present invention is achieved by the following technical programs.
Except as otherwise noted, percentage of the present invention is mass percent.
A kind of tobacco juice for electronic smoke that utilizes the preparation of delicate fragrance type tobacco leaf is made behind the raw material blending by following mass percent: delicate fragrance type cured tobacco leaf extract 10~30%, flavouring essence for tobacco 5~10%, tobacco aromatics using 1~5%, deionized water 5~10%, glycerine 10~20%, surplus is propane diols; Described delicate fragrance type cured tobacco leaf extract is selected from Yunnan delicate fragrance type cured tobacco leaf extract, a kind of in the delicate fragrance type cured tobacco leaf extract of Fujian, or their mixture.
With respect to prior art, the present invention has the following advantages:
1, tobacco juice for electronic smoke of the present invention is take the extract of delicate fragrance type tobacco leaf as main component, makes fragrance, mouthfeel and traditional delicate fragrance type cigarette more approaching of electronic cigarette.
2, tobacco juice for electronic smoke of the present invention is used for the atomizing of electronic cigarette, does not produce tar and CO, consumer's harm is reduced greatly, and the application of this product can not produce the harm of second-hand-cigarette.
The specific embodiment
The present invention is described in further detail below by embodiment, but embodiment is not limited to the technical solution.
Embodiment 1
A kind of tobacco juice for electronic smoke that utilizes the preparation of delicate fragrance type tobacco leaf, the component that comprises following mass ratio: Yunnan mountain of papers cured tobacco leaf extract 2%, Yunnan Muller cured tobacco leaf extract 1%, Yunnan Yuxi cured tobacco leaf extract 5%, Yongding County, Fujian cured tobacco leaf extract 5%, Changting, Fujian cured tobacco leaf extract 2%, Youxi County, Fujian Province cured tobacco leaf extract 3%, flavouring essence for tobacco 5%, tobacco aromatics using 3%, deionized water 7%, glycerine 18%, surplus is propane diols.Each raw material is mixed in proportion, and under normal temperature, stir 30min, make the abundant mixing of each component.
The preparation method of leaf tobacco extract is: get tobacco sample dry 1h in 40 ℃ of baking ovens, be cooled to room temperature after, pulverize with Cyclone mill.Get the 50g offal and place the 500mL triangular flask, add 250mL distilled water, extract 60min with ultrasonic wave under 45~50 ℃ condition, centrifugal 10min under the 5000rpm gets supernatant liquor and adopts the decompression rotary evaporation to be concentrated into 25mL, is leaf tobacco extract.
Described flavouring essence for tobacco mainly comprises the following composition of percentage by weight: vanillic aldehyde 0.1%, menthol 0.2%, sage clary oil 0.05%; Peru's medicinal extract 0.2%, Tolu concrete 0.05%, maltol 0.05%; cloud and mist absolute oil 0.1%, coriander seed oil 1%EA 2.5%, clove bud oil 0.1%; geranium oil 1%EA 2.5%; bay leaves oil 0.05%, iso-amyl iso-valeriate 1%EA 1.0%, 2-acetyl group pyrazine 1.0%; 2; 3,5-trimethylpyrazine 0.5%, lavender oil 1%EA 1.0%; angelica grosseserrata root tincture 3.0%; vanilla bean tincture 5.0%, red date tincture 10.0%, 3 methylvaleric acid 0.02%; propane diols 21.0%, ethanol 51.58%.Said components mixed stir 1h under the normal temperature after fitting over together.
Described tobacco aromatics using mainly comprises the following composition of percentage by weight: Fructus Monordicae extract 3%, tamarind extract 5%, locust bean extract 3%, grape seed extract 5%, apricot extract 3%, extractive of alfalfa 5%, mitral flower extract 5%, lemon oil 5%, tree moss concrete 5%, radix valerianae extract 3%, hyacinth dolichos leaf extract 4%, cherry extract 9%, apple extract 5%, deionized water 15%, propane diols 25%.Said components mixed fit over together, and in 50~60 ℃ of lower 40min that stir.
Embodiment 2
Repeat embodiment 1, following difference is arranged: utilize the tobacco juice for electronic smoke of delicate fragrance type tobacco leaf preparation, comprise the component of following mass ratio: Yunnan mountain of papers cured tobacco leaf extract 1%, Yunnan Muller cured tobacco leaf extract 1%, Yunnan Yuxi cured tobacco leaf extract 2%, Yongding County, Fujian cured tobacco leaf extract 8%, Changting, Fujian cured tobacco leaf extract 2%, Youxi County, Fujian Province cured tobacco leaf extract 3%, flavouring essence for tobacco 6%, tobacco aromatics using 5%, deionized water 6%, glycerine 18%, surplus are propane diols.
Embodiment 3
Repeat embodiment 1, following difference is arranged: utilize the tobacco juice for electronic smoke of delicate fragrance type tobacco leaf preparation, comprise the component of following mass ratio: Yunnan mountain of papers cured tobacco leaf extract 3%, Yunnan Muller cured tobacco leaf extract 2%, Yunnan Yuxi cured tobacco leaf extract 3%, Yongding County, Fujian cured tobacco leaf extract 2%, Youxi County, Fujian Province cured tobacco leaf extract 6%, Jianyang, Fujian flue-cured tobacco extract 2%, flavouring essence for tobacco 5%, tobacco aromatics using 3%, deionized water 5%, glycerine 18%, surplus are propane diols.
Embodiment 4
Repeat embodiment 1, following difference is arranged: the tobacco juice for electronic smoke that utilizes the preparation of delicate fragrance type tobacco leaf, the component that comprises following mass ratio: Qujing of Yunnan cured tobacco leaf extract 2%, Yunnan Muller cured tobacco leaf extract 2%, Yunnan Yuxi cured tobacco leaf extract 3%, Kunming, Yunnan cured tobacco leaf extract 7%, Sanming, Fujian Province cured tobacco leaf extract 2%, Yongding County, Fujian cured tobacco leaf extract 3%, Youxi County, Fujian Province cured tobacco leaf extract 1%, Jianyang, Fujian flue-cured tobacco extract 1%, flavouring essence for tobacco 6%, tobacco aromatics using 4%, deionized water 8%, glycerine 18%, surplus are propane diols.
Embodiment 5
Repeat embodiment 1, following difference is arranged: utilize the tobacco juice for electronic smoke of delicate fragrance type tobacco leaf preparation, comprise the component of following mass ratio: Kunming, Yunnan cured tobacco leaf extract 1%, Yunnan Muller cured tobacco leaf extract 2%, Yunnan Yuxi cured tobacco leaf extract 6%, Sanming, Fujian Province cured tobacco leaf extract 2%, Youxi County, Fujian Province cured tobacco leaf extract 2%, Jianyang, Fujian flue-cured tobacco extract 3%, flavouring essence for tobacco 6%, tobacco aromatics using 3%, deionized water 8%, glycerine 18%, surplus are propane diols.
Application Example 1 contrast test
The tobacco juice of embodiment 1, embodiment 2, embodiment 3, embodiment 4, embodiment 5 preparations added to carry out sensory quality assessment in the electronic cigarette, evaluation result sees Table 2.
Electronic cigarette sensory quality assessment method:
Sensory quality assessment project and scale setting: 7 projects are set, are respectively fragrance matter, perfume quantity, concentration, excitant, assorted gas, strength, pleasant impression; The maximum scale of each project is 9, and projects all are divided into the score unit with 1, sees Table 1 corresponding to the meaning of each scale value of projects.
Check problem: provide sample and check table to the expert that smokes panel test, require the person of smokeing panel test according to the form requirement indices to be smoked panel test.
Result statistics: the smoking result of all persons of smokeing panel test is all effective, and the individual event smoking result of the person of smokeing panel test is respectively asked arithmetic mean of instantaneous value, and the result remains to a decimal, and to the arithmetic mean of instantaneous value of each individual event add with, obtain total points, the result remains to a decimal.
Figure BDA0000277969451
Figure BDA0000277969452
As shown in Table 2, the tobacco juice for electronic smoke that utilizes the preparation of delicate fragrance type tobacco leaf of the present invention, because of the employed tobacco leaf place of production, extract adding proportion, flavouring essence for tobacco different with the tobacco aromatics using adding proportion, its inherent aesthetic quality is difference to some extent, and wherein the impact on fragrance matter, excitant, assorted gas and pleasant impression is larger.As seen from the above table, example 1 described formula rate structure is more rational, and aesthetic quality's score is also the highest.

Claims (1)

1. a tobacco juice for electronic smoke that utilizes the preparation of delicate fragrance type tobacco leaf is made behind the raw material blending by following mass percent: delicate fragrance type cured tobacco leaf extract 10~30%, flavouring essence for tobacco 5~10%, tobacco aromatics using 1~5%, deionized water 5~10%, glycerine 10~20%, surplus is propane diols; Described delicate fragrance type cured tobacco leaf extract is selected from Yunnan delicate fragrance type cured tobacco leaf extract, a kind of in the delicate fragrance type cured tobacco leaf extract of Fujian, or their mixture.
CN2013100297032A 2013-01-25 2013-01-25 Electronic cigarette tobacco juice prepared from faint scent tobacco leaves Pending CN103070473A (en)

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Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103622154A (en) * 2013-12-17 2014-03-12 郑悦 Electronic cigarette liquid and preparation method thereof
CN103653235A (en) * 2013-12-16 2014-03-26 红塔烟草(集团)有限责任公司 Atomized cigarette liquid of electronic cigarette and preparation method
CN103932382A (en) * 2014-03-12 2014-07-23 红塔烟草(集团)有限责任公司 Fresh scent electronic cigarette nicotine liquid and preparation method thereof
CN104082855A (en) * 2014-07-28 2014-10-08 嘉兴市得百科新材料科技有限公司 Double-apple-aroma electronic cigarette liquid and preparation method thereof
CN104432489A (en) * 2014-10-22 2015-03-25 浙江中烟工业有限责任公司 Electronic cigarette tobacco juice solvents utilizing polyglycerol and electronic cigarette tobacco juice and electronic cigarette prepared through electronic cigarette tobacco juice solvents
CN104489900A (en) * 2014-11-26 2015-04-08 浙江中烟工业有限责任公司 Mint-flavored nicotine liquid and electronic cigarette with same
CN104489907A (en) * 2014-12-17 2015-04-08 贵州中烟工业有限责任公司 Sauce-fragrance E-cigarette nicotine liquid
CN104489905A (en) * 2014-12-17 2015-04-08 贵州中烟工业有限责任公司 Liquor-fragrance E-cigarette nicotine liquid
CN104585860A (en) * 2015-01-15 2015-05-06 中国烟草总公司郑州烟草研究院 Preparation method for electronic cigarette juice having baking fragrant characteristic
CN104585869A (en) * 2015-01-20 2015-05-06 川渝中烟工业有限责任公司 Electronic cigarette liquid containing glucoside
CN104585868A (en) * 2015-01-20 2015-05-06 川渝中烟工业有限责任公司 Human body essential amino acid-rich electronic cigarette juice
CN105725259A (en) * 2016-03-10 2016-07-06 四川中烟工业有限责任公司 Heavy cigar-type electronic cigarette and preparation method thereof
CN110464043A (en) * 2019-07-09 2019-11-19 河南中烟工业有限责任公司 For heating the faint scent essence and reconstituted tobacoo and the cigarette that do not burn of the cigarette that do not burn
CN111227295A (en) * 2020-01-20 2020-06-05 深圳梵活生命科学股份有限公司 Smokeless electronic atomized liquid and preparation method thereof
CN113749278A (en) * 2021-09-16 2021-12-07 深圳市真味生物科技有限公司 Lily-flavored electronic atomized liquid and preparation method thereof

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CN102813278A (en) * 2012-08-09 2012-12-12 深圳瀚星翔科技有限公司 Mixed electronic cigarette tobacco liquid

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Cited By (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103653235A (en) * 2013-12-16 2014-03-26 红塔烟草(集团)有限责任公司 Atomized cigarette liquid of electronic cigarette and preparation method
CN103622154A (en) * 2013-12-17 2014-03-12 郑悦 Electronic cigarette liquid and preparation method thereof
CN103932382A (en) * 2014-03-12 2014-07-23 红塔烟草(集团)有限责任公司 Fresh scent electronic cigarette nicotine liquid and preparation method thereof
CN104082855B (en) * 2014-07-28 2015-10-21 嘉兴市得百科新材料科技有限公司 Electronic cigarette liquid of a kind of pair of apple local flavor and preparation method thereof
CN104082855A (en) * 2014-07-28 2014-10-08 嘉兴市得百科新材料科技有限公司 Double-apple-aroma electronic cigarette liquid and preparation method thereof
CN104432489A (en) * 2014-10-22 2015-03-25 浙江中烟工业有限责任公司 Electronic cigarette tobacco juice solvents utilizing polyglycerol and electronic cigarette tobacco juice and electronic cigarette prepared through electronic cigarette tobacco juice solvents
CN104432489B (en) * 2014-10-22 2016-03-30 浙江中烟工业有限责任公司 A kind ofly utilize the tobacco juice for electronic smoke solvent of polyglycerol and the tobacco juice for electronic smoke of preparation thereof and electronic cigarette
CN104489900A (en) * 2014-11-26 2015-04-08 浙江中烟工业有限责任公司 Mint-flavored nicotine liquid and electronic cigarette with same
CN104489907A (en) * 2014-12-17 2015-04-08 贵州中烟工业有限责任公司 Sauce-fragrance E-cigarette nicotine liquid
CN104489905A (en) * 2014-12-17 2015-04-08 贵州中烟工业有限责任公司 Liquor-fragrance E-cigarette nicotine liquid
CN104585860B (en) * 2015-01-15 2016-11-30 中国烟草总公司郑州烟草研究院 There is the preparation method of the tobacco juice for electronic smoke of the fragrant feature of baking
CN104585860A (en) * 2015-01-15 2015-05-06 中国烟草总公司郑州烟草研究院 Preparation method for electronic cigarette juice having baking fragrant characteristic
CN104585868A (en) * 2015-01-20 2015-05-06 川渝中烟工业有限责任公司 Human body essential amino acid-rich electronic cigarette juice
CN104585869B (en) * 2015-01-20 2016-02-03 川渝中烟工业有限责任公司 A kind of tobacco juice for electronic smoke containing glucosides
CN104585869A (en) * 2015-01-20 2015-05-06 川渝中烟工业有限责任公司 Electronic cigarette liquid containing glucoside
CN105725259A (en) * 2016-03-10 2016-07-06 四川中烟工业有限责任公司 Heavy cigar-type electronic cigarette and preparation method thereof
CN110464043A (en) * 2019-07-09 2019-11-19 河南中烟工业有限责任公司 For heating the faint scent essence and reconstituted tobacoo and the cigarette that do not burn of the cigarette that do not burn
CN110464043B (en) * 2019-07-09 2022-01-11 河南中烟工业有限责任公司 Fragrant essence for heating non-combustible cigarette, tobacco sheet and non-combustible cigarette
CN111227295A (en) * 2020-01-20 2020-06-05 深圳梵活生命科学股份有限公司 Smokeless electronic atomized liquid and preparation method thereof
CN113749278A (en) * 2021-09-16 2021-12-07 深圳市真味生物科技有限公司 Lily-flavored electronic atomized liquid and preparation method thereof
CN113749278B (en) * 2021-09-16 2023-09-12 深圳市真味生物科技有限公司 Lily-flavored electronic atomized liquid and preparation method thereof

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Application publication date: 20130501