CN104082855A - Double-apple-aroma electronic cigarette liquid and preparation method thereof - Google Patents
Double-apple-aroma electronic cigarette liquid and preparation method thereof Download PDFInfo
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- CN104082855A CN104082855A CN201410360458.8A CN201410360458A CN104082855A CN 104082855 A CN104082855 A CN 104082855A CN 201410360458 A CN201410360458 A CN 201410360458A CN 104082855 A CN104082855 A CN 104082855A
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Abstract
The invention provides double-apple-aroma electronic cigarette liquid and a preparation method of the double-apple-aroma electronic cigarette liquid. The double-apple-aroma electronic cigarette liquid is formed by evenly mixing propylene glycol, glycerin, 1,3-butanediol, xylitol liquid, green apple extracts, edible apple essence and others according to the proportion. The green apple extracts are obtained with ethyl alcohol through performing heating, reflux extraction, pressure reduction rotary evaporation and concentration. The double-apple-aroma electronic cigarette liquid comprises, by weight, 1-80 parts of propylene glycol, 1-70 parts of glycerin, 1-50 parts of 1,3-butanediol, 1-30 parts of xylitol liquid, 1-20 parts of green apple extracts and 0.1-5 parts of edible apple essence. The electronic cigarette liquid is good in double apple aroma and fresh and sweet in taste and can meet the requirements for smoking an apple-aroma electronic cigarette for consumers.
Description
Technical field
The invention belongs to flavouring essence for tobacco field, relate to a kind of electronic cigarette liquid and preparation method thereof, particularly relate to electronic cigarette liquid of a kind of pair of apple local flavor and preparation method thereof.
Technical background
Electronic cigarette is a kind of Miniature atomized device that adopts high-new microelectric technique, is the substitute of conventional cigarette.Electronic cigarette does not have other harmful components such as tar, suspended particulates in cigarette, produces hardly second-hand-cigarette yet.Electronic cigarette is generally made up of three parts: tobacco rod, atomizer and cigarette bullet.In the time that smoker is air-breathing by cigarette holder, the electronic cigarette liquid in cigarette bullet is the heated droplet that is atomized into 0.5-1.5um left and right in atomizer, forms simulation smoke.
Fragrance and the mouthfeel of electronic cigarette derive from electronic cigarette liquid, and the composition of electronic cigarette liquid is mainly essence and flavoring agent, tobacco extract and propane diols, glycerine equal solvent.At present, fruity electronic cigarette relies on its fresh and sweet various taste to be subject to consumers in general's favor.
Summary of the invention
the technical problem solving:apple is liked by consumer deeply as a kind of Common Fruits, have the product of numerous apple aromas on market, and apple local flavor electronic cigarette is also one of modal product on electronic cigarette market.But the general fragrance of apple aroma electronic cigarette is in the market single, mouthfeel is sweet greasy, and pleasant impression is unclean, can not meet consumer's requirement of sense.
technical scheme:for above-mentioned technical problem, the invention discloses the electronic cigarette liquid of a kind of pair of apple local flavor, the electronic cigarette liquid of described two apple local flavors consists of the following composition: propane diols, glycerine, 1,3-BDO, xylitol liquid, green apple extract and edible flavoring apple essence.
Preferably, in the electronic cigarette liquid of a kind of pair of described apple local flavor, the parts by weight of each component are: propane diols 1-80 part, glycerine 1-70 part, 1,3-BDO 1-50 part, xylitol liquid 1-30 part, green apple extract 1-20 part, edible flavoring apple essence 0.1-5 part.
Preferably, the electronic cigarette liquid of a kind of pair of described apple local flavor is sundown.
Preferably, the electronic cigarette liquid of a kind of pair of described apple local flavor, described edible flavoring apple essence is composed of the following components: iso-amyl iso-valeriate, ethyl isovalerate, isoamyl butyrate, ethyl acetate, vanillic aldehyde, benzaldehyde, citral, isoamyl formate, geranium oil, allyl hexanoate, caryophyllus oil, 95% ethanol and distilled water.
Iso-amyl iso-valeriate 1-8 part, ethyl isovalerate 0.1-2 part, isoamyl butyrate 0.1-2 part, ethyl acetate 0.1-2 part, vanillic aldehyde 0.1-1 part, benzaldehyde 0.01-1 part, citral 0.01-1 part, isoamyl formate 0.1-2 part, geranium oil 0.01-1 part, allyl hexanoate 0.01-1 part, caryophyllus oil 0.01-1 part, 95% ethanol 30-90 part, distilled water 10-50 part.
Preferably, the electronic cigarette liquid of a kind of pair of described apple local flavor, in described edible two flavoring apple essences, the parts by weight of each component are: iso-amyl iso-valeriate 1-8 part, ethyl isovalerate 0.1-2 part, isoamyl butyrate 0.1-2 part, ethyl acetate 0.1-2 part, vanillic aldehyde 0.1-1 part, benzaldehyde 0.01-1 part, citral 0.01-1 part, isoamyl formate 0.1-2 part, geranium oil 0.01-1 part, allyl hexanoate 0.01-1 part, caryophyllus oil 0.01-1 part, 95% ethanol 30-90 part, distilled water 10-50 part.
Preferably, the electronic cigarette liquid of a kind of pair of described apple local flavor, described green apple extract is with the green apple extract obtaining after alcohol extract.
Preferably, described green apple method for preparing extractive comprises the following steps: (1) takes clean green apple, smashs to pieces with tissue mashing machine; (2) add in proportion certain density ethanol, ultrasonic wave extracts three times; (3) merge extract, decompression rotary evaporation is condensed into paste, for subsequent use.
Preferably, in the preparation method of described tomato extract, concentration of alcohol used is 60wt% ~ 90wt%, solid-liquid ratio is 1:8-1:20, supersonic frequency is 50 ~ 400kHz, ultrasonic power is 50 ~ 600W, ultrasonic extraction time of single is 10-30min, and the concentrated temperature of decompression rotary evaporation is 50 DEG C, and vacuum is 0.095 Mpa.
A preparation method for the electronic cigarette liquid of pair apple local flavor, comprises the steps: that (1) takes clean green apple, smashs to pieces with tissue mashing machine; (2) add ethanol, ultrasonic wave extracts three times, and concentration of alcohol is 60wt% ~ 90wt%, and solid-liquid ratio is 1:8-1:20, and supersonic frequency is 50 ~ 400kHz, and ultrasonic power is 50 ~ 600W, and ultrasonic extraction time of single is 10-30min; (3) merge extract, decompression rotary evaporation is condensed into paste, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, concentrated rear for subsequent use; (4) get iso-amyl iso-valeriate 1-8 part, ethyl isovalerate 0.1-2 part, isoamyl butyrate 0.1-2 part, ethyl acetate 0.1-2 part, vanillic aldehyde 0.1-1 part, benzaldehyde 0.01-1 part, citral 0.01-1 part, isoamyl formate 0.1-2 part, geranium oil 0.01-1 part, allyl hexanoate 0.01-1 part, caryophyllus oil 0.01-1 part, 95% ethanol 30-90 part, distilled water 10-50 part, obtains edible flavoring apple essence after mentioned component is mixed; (5) get propane diols 1-80 part, glycerine 1-70 part, 1,3-BDO 1-50 part, xylitol liquid 1-30 part, green apple extract 1-20 part, edible flavoring apple essence 0.1-5 part, after mentioned component is mixed, prepare the electronic cigarette liquid of two apple local flavors.
The xylitol aqueous solution that described xylitol liquid is 20wt% to 40wt%.
beneficial effect:the electronic cigarette liquid of the two apple local flavors that prepare by preparation method of the present invention is sundown, overcome that the general fragrance of apple aroma electronic cigarette is single, mouthfeel is sweet greasy, pleasant impression is unclean, can not meet the shortcoming of consumer's requirement of sense, electronic cigarette liquid of the present invention can provide salubrious green apple fragrance and sweet apple fragrance in the time of suction, mouthfeel is soft and moist and pleasant impression is totally comfortable, and the preparation method of described electronic cigarette liquid is easy, constant product quality, can be widely used in electronic cigarette product.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described.
Embodiment 1
(1) take clean green apple, smash to pieces with tissue mashing machine; Add ethanol, ultrasonic wave extracts three times, and concentration of alcohol is 70wt%, and solid-liquid ratio is 1:15, and supersonic frequency is 400kHz, and ultrasonic power is 600W, and ultrasonic extraction time of single is 15min; Merge extract, decompression rotary evaporation is condensed into paste, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, concentrated rear for subsequent use;
(2) get by weight 5 parts of iso-amyl iso-valeriates, 1.2 parts of ethyl isovalerates, 1.5 parts of isoamyl butyrates, 1 part, ethyl acetate, 0.1 part of vanillic aldehyde, 0.01 part of benzaldehyde, 0.06 part of citral, 0.6 part of isoamyl formate, 0.01 part of geranium oil, 0.01 part of allyl hexanoate, 0.05 part of caryophyllus oil, 70 parts of 95% ethanol, 20 parts of distilled water, obtain edible flavoring apple essence after mentioned component is mixed;
(3) get by weight 0.1 part of 55 parts of propane diols, 15 parts of glycerine, 15 parts of 1,3-BDOs, 5 parts of the xylitol liquid of 20wt%, 9.8 parts of green apple extracts, edible flavoring apple essence and mix, obtain the electronic cigarette liquid of two apple local flavors.
Embodiment 2
(1) take clean green apple, smash to pieces with tissue mashing machine; Add ethanol, ultrasonic wave extracts three times, and concentration of alcohol is 90wt%, and solid-liquid ratio is 1:8, and supersonic frequency is 50kHz, and ultrasonic power is 50W, and ultrasonic extraction time of single is 30min; Merge extract, decompression rotary evaporation is condensed into paste, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, concentrated rear for subsequent use;
(2) get by weight 8 parts of iso-amyl iso-valeriates, 2 parts of ethyl isovalerates, 0.1 part of isoamyl butyrate, 0.1 part, ethyl acetate, 0.3 part of vanillic aldehyde, 0.05 part of benzaldehyde, 0.01 part of citral, 0.1 part of isoamyl formate, 0.5 part of geranium oil, 0.05 part of allyl hexanoate, 1 part of caryophyllus oil, 30 parts of 95% ethanol, 10 parts of distilled water, obtain edible flavoring apple essence after mentioned component is mixed;
(3) get by weight 5 parts of 1 part of propane diols, 70 parts of glycerine, 50 parts of 1,3-BDOs, 1 part of 40wt% xylitol liquid, 1 part of green apple extract, edible flavoring apple essences and mix, obtain the electronic cigarette liquid of two apple local flavors.
Embodiment 3
(1) take clean green apple, smash to pieces with tissue mashing machine; Add ethanol, ultrasonic wave extracts three times, and concentration of alcohol is 60wt%, and solid-liquid ratio is 1:20, and supersonic frequency is 200kHz, and ultrasonic power is 300W, and ultrasonic extraction time of single is 10min; Merge extract, decompression rotary evaporation is condensed into paste, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, concentrated rear for subsequent use;
(2) get by weight 1 part of iso-amyl iso-valeriate, 0.1 part of ethyl isovalerate, 2 parts of isoamyl butyrates, 2 parts, ethyl acetate, 1 part of vanillic aldehyde, 1 part of benzaldehyde, 1 part of citral, 2 parts of isoamyl formates, 1 part of geranium oil, 1 part of allyl hexanoate, 0.01 part of caryophyllus oil, 90 parts of 95% ethanol, 50 parts of distilled water, obtain edible flavoring apple essence after mentioned component is mixed;
(3) get by weight 0.5 part of 80 parts of propane diols, 1 part of glycerine, 1 part of 1,3-BDO, 30 parts of the xylitol liquid of 30wt%, 20 parts of green apple extracts, edible flavoring apple essence and mix, obtain the electronic cigarette liquid of two apple local flavors.
Two apple local flavor electronic cigarette liquids of the embodiment preparing 1, embodiment 2, embodiment 3 are got to 0.5mL to be added in electronic cigarette, and separately get commercially available edible flavoring apple essence propane diols and be diluted to after 0.3wt%, the commercially available edible flavoring apple essence dilution of 0.3wt% of getting 0.5mL is added in electronic cigarette, as a comparison case, carry out comprehensive sensory quality assessment.Result is as follows:
Embodiment 1: flue gas is full, apple gives off a strong fragrance and be rich in stereovision, mouthfeel sweet soft, pleasant impression is comfortable.
Embodiment 2: flue gas is strong, apple fragrance is soft and moist and be rich in stereovision, mouthfeel is fresh and sweet exquisiteness, pleasant impression be clean.
Embodiment 3: flue gas is strong, apple fragrance is soft and it is clean to be rich in stereovision, delicate mouthfeel, pleasant impression.
Comparative example: flue gas is strong, apple fragrance coordinate, mouthfeel sweet greasy, pleasant impression is not good enough.
From result, can find out, the green apple fragrance that the electronic cigarette liquid of the two apple local flavors that prepare by preparation method of the present invention is salubrious and sweet apple fragrance, mouthfeel is soft and moist and pleasant impression is totally comfortable, and the preparation method of described electronic cigarette liquid is easy, constant product quality, can be widely used in electronic cigarette product.
Claims (8)
1. an electronic cigarette liquid for two apple local flavors, is characterized in that the electronic cigarette liquid of described two apple local flavors consists of the following composition: propane diols, glycerine, 1,3-BDO, xylitol liquid, green apple extract and edible flavoring apple essence.
2. the electronic cigarette liquid of a kind of pair of apple local flavor according to claim 1, in the electronic cigarette liquid of the two apple local flavors described in it is characterized in that, the parts by weight of each component are: propane diols 1-80 part, glycerine 1-70 part, 1,3-BDO 1-50 part, xylitol liquid 1-30 part, green apple extract 1-20 part, edible flavoring apple essence 0.1-5 part.
3. the electronic cigarette liquid of a kind of pair of apple local flavor according to claim 1, is characterized in that described electronic cigarette liquid is sundown.
4. the electronic cigarette liquid of a kind of pair of apple local flavor according to claim 1, is characterized in that described edible flavoring apple essence is composed of the following components: iso-amyl iso-valeriate, ethyl isovalerate, isoamyl butyrate, ethyl acetate, vanillic aldehyde, benzaldehyde, citral, isoamyl formate, geranium oil, allyl hexanoate, caryophyllus oil, 95% ethanol and distilled water.
5. the electronic cigarette liquid of a kind of pair of apple local flavor according to claim 1, the parts by weight that it is characterized in that each component in described edible flavoring apple essence are: iso-amyl iso-valeriate 1-8 part, ethyl isovalerate 0.1-2 part, isoamyl butyrate 0.1-2 part, ethyl acetate 0.1-2 part, vanillic aldehyde 0.1-1 part, benzaldehyde 0.01-1 part, citral 0.01-1 part, isoamyl formate 0.1-2 part, geranium oil 0.01-1 part, allyl hexanoate 0.01-1 part, caryophyllus oil 0.01-1 part, 95% ethanol 30-90 part, distilled water 10-50 part.
6. the electronic cigarette liquid of a kind of pair of apple local flavor according to claim 1, is characterized in that the preparation method of described green apple extract comprises the following steps: (1) takes clean green apple, smashs to pieces with tissue mashing machine; (2) add in proportion certain density ethanol, ultrasonic wave extracts three times; (3) merge extract, decompression rotary evaporation is condensed into paste, for subsequent use.
7. the electronic cigarette liquid of a kind of pair of apple local flavor according to claim 6, it is characterized in that in the preparation method of green apple extract, concentration of alcohol used is 60wt% ~ 90wt%, solid-liquid ratio is 1:8-1:20, supersonic frequency is 50 ~ 400kHz, ultrasonic power is 50 ~ 600W, ultrasonic extraction time of single is 10-30min, and the concentrated temperature of decompression rotary evaporation is 50 DEG C, and vacuum is 0.095 Mpa.
8. a preparation method for the electronic cigarette liquid of two apple local flavors, is characterized in that comprising the steps: that (1) takes clean blue or green tomato, smashs to pieces with tissue mashing machine; (2) add ethanol, ultrasonic wave extracts three times, and concentration of alcohol is 60wt% ~ 90wt%, and solid-liquid ratio is 1:8-1:20, and supersonic frequency is 50 ~ 400kHz, and ultrasonic power is 50 ~ 600W, and ultrasonic extraction time of single is 10-30min; (3) merge extract, decompression rotary evaporation is condensed into paste, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, concentrated rear for subsequent use; (4) get iso-amyl iso-valeriate 1-8 part, ethyl isovalerate 0.1-2 part, isoamyl butyrate 0.1-2 part, ethyl acetate 0.1-2 part, vanillic aldehyde 0.1-1 part, benzaldehyde 0.01-1 part, citral 0.01-1 part, isoamyl formate 0.1-2 part, geranium oil 0.01-1 part, allyl hexanoate 0.01-1 part, caryophyllus oil 0.01-1 part, 95% ethanol 30-90 part, distilled water 10-50 part, obtains edible flavoring apple essence after mentioned component is mixed; (5) get propane diols 1-80 part, glycerine 1-70 part, 1,3-BDO 1-50 part, xylitol liquid 1-30 part, green apple extract 1-20 part, edible flavoring apple essence 0.1-5 part; After being mixed, mentioned component prepares the electronic cigarette liquid of two apple local flavors.
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| CN201410360458.8A CN104082855B (en) | 2014-07-28 | 2014-07-28 | Electronic cigarette liquid of a kind of pair of apple local flavor and preparation method thereof |
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| CN201410360458.8A CN104082855B (en) | 2014-07-28 | 2014-07-28 | Electronic cigarette liquid of a kind of pair of apple local flavor and preparation method thereof |
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| CN104382223A (en) * | 2014-10-22 | 2015-03-04 | 浙江中烟工业有限责任公司 | Solvent suitable for preparation of fruity nicotine liquid, and nicotine liquid and electronic cigarette prepared by solvent |
| CN104585862A (en) * | 2015-01-15 | 2015-05-06 | 云南中烟工业有限责任公司 | Sweet greasiness-free tobacco juice of electronic cigarette |
| CN107460041A (en) * | 2016-06-04 | 2017-12-12 | 沈百祥 | A kind of flavoring apple essence preparation method |
| CN107581655A (en) * | 2017-08-29 | 2018-01-16 | 深圳市真味生物科技有限公司 | A kind of compound dry electronic cigarette tobacco tar and preparation method thereof |
| CN115067540A (en) * | 2022-07-11 | 2022-09-20 | 湖北中烟工业有限责任公司 | Apple extract for cigarettes and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115067540A (en) * | 2022-07-11 | 2022-09-20 | 湖北中烟工业有限责任公司 | Apple extract for cigarettes and preparation method thereof |
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| CN104082855B (en) | 2015-10-21 |
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